modification of poly(ethylene terephthalate) fiber by grafting of acrylic acid/acrylamid for removel of pb+2 from aqueous solutions

Authors

majid abdouss

homayon ahmad panahi

forozan ghiabi,

elham moniri,

ahmad mousavi shoushtari

abstract

: a new fibrous adsorbent was prepared by grafting acrylic acid /acryl amide (aa/aam) co-monomers onto poly(ethylene terephtalat) (pet) fibers. the resulting sorbent has been characterized by fourier transform infrared spectroscopy (ft-ir), thermo gravimetric analysis (tga), scanning electron microscopy (sem) and elemental analysis and studied for the preconcentration and determination of trace pb+2 ion from water sample. the effects of reaction conditions such as monomer mixture ratio, grafting yield, polymerization. the time and temperature on grafting were investigated. batch adsorption method was used for the  pre concentration studies. recovery of pb+2 was 100.2% at optimum conditions. the adsorption capacity of the adsorbent was found 44.1mg/gforpb+2.

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Journal title:
iranian journal of chemistry and chemical engineering (ijcce)

Publisher: iranian institute of research and development in chemical industries (irdci)-acecr

ISSN 1021-9986

volume 31

issue 1 2012

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